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Derivatives of 9‐phenyl‐9H‐carbazole were synthesized as efficient emitters exhibiting both thermally activated delayed fluorescence and aggregation‐induced emission enhancement. Effects of methoxy and tert‐butyl substituents at the different positions of carbazolyl groups on the properties of the emitters were studied. Depending on the substitutions, photoluminescence quantum yields (PLQY) of non‐doped...