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The present work provides a novel process for the preparation of abiraterone drug in a Suzuki–Miyaura coupling approach by a new heterogeneous palladium catalyst, Pd‐NPs@Zn‐MOF, which has been synthesized by one‐step encapsulation in nanoporous metal–organic framework Zn‐MOF under a temperature control program for the first time. Pd‐NPs@Zn‐MOF were characterized by transmission electron microscopy...