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The asymmetric Salamo‐type N2O2 ligand H2L and its corresponding CuII and ZnII complexes [CuL] and [{ZnL}2]·2CH3CN were synthesized and structurally characterized. Crystallographic data of the CuII complex revealed that the CuII ion is tetracoordinate with a slightly distorted square planar arrangement forming a 2D supramolecular plane structure by hydrogen bonding and π···π stacking interactions...
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