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A multi‐molybdate coordination‐polymer‐precursor route was developed to synthesize mesoporous MoO3 nanoribbons. In this reaction process, the coordination‐polymer‐precursor (i.e., {Mo36} ions) was firstly synthesized, as proven by FTIR spectroscopy. By controlling the experimental conditions, the {Mo36} ions underwent a directed assembly process and a dehydration process to form 1D mesoporous MoO3...
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