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Layered double hydroxides with a high layer charge (+0.33 per empirical formula unit) intercalate nitrate ions with the molecular plane of the NO3– ion inclined at ca. 70° to the metal hydroxide layer, which results in a basal spacing of 8.8 Å. Three different N–O bond lengths are observed and yield Cs coordination symmetry. At lower charge (0.165 ≤ x ≤ 0.2), a basal spacing of 8.0 Å is observed,...
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