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Three novel diiron azadithiolate complexes Fe2[(μ-SCH2)2NCH2CH2CH(CH3)2](CO)6 (1), Fe2[(μ-SCH2)2NCH(CH2CH3)2](CO)6 (2) and Fe2[(μ-SCH2)2NCH2CH2CH2SCH3](CO)6 (3) have been synthesized by treatment of Fe2(μ-SCH2OH)2(CO)6 with primary amines RNH2 (R=CH2CH2CH(CH3)2, CH(CH2CH3)2, CH2CH2CH2SCH3). Meanwhile, reaction of Fe2(μ-SCH2OH)2(CO)6 and diphosphine ligand Ph2PCH2PPh2 (dppm), followed by the addition...
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