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Five diiron ethanedithiolate complexes bearing acetate ester have been prepared and characterized. Esterification of complex [{μ-SCH2CH(CH2OH)S}Fe2(CO)6] (1) with acetic acid in the presence of N,N′-dicyclohexylcarbodiimide and 4-dimethylaminopyridine gave the acetate ester [{μ-SCH2CH(CH2O2CCH3)S}Fe2(CO)6] (2) in 94% yield. Further treatment of complex 2 with a monophosphine ligand triphenylphosphine,...
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