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In this paper, two crystalline-coil diblock copolymers consisting of blocks of syndiotactic polypropylene (sPP) with different syndiotacticities ([rrrr]sPP1 = 0.78, [rrrr]sPP2 = 0.94) and poly(ethylene oxide) (PEO) were synthesized utilizing the click reaction of azide-terminated PEO (PEO–N3) with alkynyl-terminated sPP (sPP–C≡CH), which was obtained via the syndiospecific polymerization of propylene...
This study demonstrates the self-assembly of crystalline-coil diblock copolymers of poly(ε-caprolactone)-b-poly(ethylene oxide) (PCL-b-PEO) with narrow molecular weight distributions in aqueous solution. The formed spherical micelles with sub-100 nm diameters are composed of a PCL core with low crystallinity and a soluble PEO corona. Isothermal crystallization behavior of the core-forming PCL blocks...
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