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Fluorinated phases formed by reaction of Fe0.5Co0.5Sb2O4 and Fe0.5Mg0.5Sb2O4 with gaseous fluorine have been examined by 57 Fe Mössbauer spectroscopy between 298 and 5 K. The degree of oxidation of Fe2+to Fe3 +has been used to quantify the amount of fluorine incorporated within the channels of the schafarzikite-related structure and enable the evaluation of the compositions as Fe0.5Co0.5Sb2O4F0.41...
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