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Hydrodynamic structuring of alkoxide-based sols in an electrical field is a promising technique to fabricate one-dimensional materials as free-standing fiber mats with high surface area and precisely controlled microstructure. Hollow α-LiFeO2 and composite α-LiFeO2/C nanofibers were prepared as self-supported 3D architectures of ceramic fibers by single-step electrospinning of metal alkoxide sols...