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A facile solvothermal sulfurization using electro-oxidized nickel foam (NF(Ox)) as support has been applied to prepare NiSx/NF(Ox) electrocatalyst with highly efficient activity for oxygen evolution reaction (OER). XRD patterns confirm the composition of NiSx/NF(Ox): two kinds of crystal phase including β-NiS and Ni3S2. While using bare NF as support under identical conditions, only Ni3S2 phase can...
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