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Mesoporous carbon nitride (MCN) has been prepared through a simple polymerization reaction between ethylenediamine (EDA) and carbon tetrachloride (CTC) by a nano hard-templating approach. The obtained MCN possesses high surface area (166.3m2/g), average pore size of 9.2nm and high N content (up to 18.5wt%). The negative charge and the basicity on MCN surface are originated from its rich carbon nitride...