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Crystallization mechanism of sol‐gel synthesized spinel LiMn2O4 is studied by a differential scanning calorimetry (DSC) method. Lithium acetate and manganese acetate are dissolved in methanol in the atomic ratio of 1:2 (Li:Mn) with citric acid as a chelating agent, leading to a sol solution. A Li‐Mn gel precursor is obtained by partly evaporating the sol solution. A large exothermic reaction of the...
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