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The halogenopentacarbonylrhenium(I) compounds react with 2,6-bis(diphenylphosphinosulfide) pyridine (L) under mild conditions to yield ionic complexes of general formulae, fac-[Re(CO) 3 L] + [Re 2 (CO) 6 (μ-X) 3 ] - (X=Cl, Br or I), in which the ligand adopts a facial terdentate bonding mode. A synthesis of [Re(CO) 3 L] + [SbF 6 ...
Reaction of pentane-2,4-dione, pyridine-2-carboxylic acid or pyridine-2,6-dicarboxylic acid with trimethylplatinum(IV) gives dimeric complexes of general formulae fac-[PtMe 3 L] 2 , in which the ionised ligand acts in a chelating and a bridging fashion. High-resolution solid-state 19 ;Pt NMR data shows that the two platinum atoms are equivalent ; the chemical shielding anisotropy...
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