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The effect that the titania doping and the sintering temperature has on the relationship between the titanium local environment and the electrical properties of YSZ has been studied. To this end, materials obtained for different titania additions ranging from 5 to 30 mol%, and sintered at different temperatures, have been studied. The combined results obtained by XRD, FT-Raman, and FE-SEM-EDX clearly...
This work reports a real-time structural study of the synthesis of zinc oxide (ZnO) capped nanoparticles (NPs) by sol-gel method. The experimental set-up developed in order to perform the in-situ X-ray absorption spectroscopy (XAS) is fully described, as well as the initial results. The size, crystallinity and short range order of the NPs was investigated, focusing on the timedependence of the process...
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