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The rotational spectrum of HCCCN-SO 3 has been observed using Fourier transform microwave spectroscopy. The vibrationally averaged structure is that of a symmetric top, with the HCCCN axis along the C 3 axis of the SO 3 , and the nitrogen end near the sulfur. The N-S bond length is 2.567(13) Å, which is slightly shorter than the sum of the van der Waals radii. The NSO angle...
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