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The route via the cross‐linking of hyperbranched prepolymers has potential advantage to construct low dielectric constant (low‐k) resins owing to the enhanced molecular free volume in hyperbranched structure. However, it is still a challenge to prepare hyperbranched resins with good film‐forming property and low‐k. In this paper, two hyperbranched polycarbosilanes with reactive benzocyclobutene groups...
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