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A straightforward synthesis of Salalens, tetradentate [ONNO]-type ligands comprised of an amine-phenolate and an imine-phenolate subunits is introduced. The Salalen ligand precursor reacted with titanium(IV) ethoxide and with tetrakis(dimethylamido)zirconium to yield the corresponding [(Salalen)MX 2 ]-type C 1 -symmetric complexes in a single isomeric form, indicating that Salalen...
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