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Tandem mass spectrometry of co-oligomers composed of methacrylic acid (MAA) and methyl methacrylate (MMA) units was performed after activated electron photo-detachment dissociation (activated EPD). In this technique, doubly charged MAA/MMA co-oligomers were first produced in negative mode electrospray ionization. Species produced upon electron photo-detachment (220nm) of these doubly charged co-oligomers...
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