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Mononuclear MnIII–peroxo and dinuclear bis(μ‐oxo)MnIII2 complexes that bear a common macrocyclic ligand were synthesized by controlling the concentration of the starting MnII complex in the reaction of H2O2 (i.e., a MnIII–peroxo complex at a low concentration (≤1 mM) and a bis(μ‐oxo)MnIII2 complex at a high concentration (≥30 mM)). These intermediates were successfully characterized by various physicochemical...
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