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Continuous synthesis of silver nanoparticles was successfully achieved using a novel counter-current pipe in pipe hydrothermal reactor. Aqueous solutions of silver acetate (99% Sigma Aldrich) were flowed in aqueous solutions with concentrations of 0.0005M to 0.03M. Supercritical conditions were shown to be necessary to produce detectable quantities of products. The conversion of the metal precursor...
Cubic Co 3 O 4 nanoparticles have been produced hydrothermally by mixing high temperature water (sub-, near to supercritical) with an aqueous cobalt acetate precursor at high pressure. The relationship between operating variables such as synthesis temperature and residence time on particle size and conversion rate was examined. An increasing nanoparticle size was observed when synthesis...
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