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In situ time-resolved X-ray diffraction (TR-XRD) using synchrotron radiation has been used to capture the dynamics of the reduction of nanocrystalline CuO using a normal supply of CO gas. Copper(II) oxide nanoparticles 4–16nm in width, as measured by XRD peak broadening, are synthesized using an aqueous organic-nitrate method and reduced in isothermal and temperature ramping reduction experiments...
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