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Tetraamine Me6TREN has been used as a scaffold support to provide coordinative saturation in the complexes PhCH2M⋅Me6TREN (M=Li, Na, K). The Li derivative displays a LiC σ interaction with a pyramidalized CH2 both in the solid state and in solution, and represents the first example of η4 coordination of Me6TREN to lithium. In the sodium derivative, the metal cation slips slightly towards the delocalized...
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