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The geometry of a series of carbon iodides have been determined, CI4 by gas-phase electron diffraction and CIn (n = 1–4) and C2I2n (n = 1–3) by high-level quantum chemical calulations. The bond length of the tetrahedral CI4 molecule from electron diffraction is (rg):2.157(10) Å. The indication of about 20% I2 in the vapor suggests partial decomposition and it has been thoroughly investigated what...
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