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Porous layered solids can be prepared by the vacuum sublimation of the ferrous porphyrin complexes Fe(Por) onto a CaF 2 or KBr substrate in a cryostat. The facile reactions of these heme models with volatile reactants can be studied in detail using FTIR and optical spectroscopy. The power of this technique draws from the ability to investigate such processes under carefully controlled and...
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