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In this work, we report the preparation and properties of Au-based cavity-microelectrodes. The use of gold as cavity current collector allows obtaining a regular cylindrical recess, whose volume is easily determined with good accuracy and precision. This in turn leads to an improved and much more reliable use of the cavity microelectrode (C-ME) as a tool for the quantitative characterization of finely...
In this work, we show our most recent results on the reductive dehalogenation of organic chlorides in acetonitrile + water media on silver electrodes, whose impressive catalytic power toward this reaction have already been extensively demonstrated and discussed. We adopt benzyl chloride as model molecule because of its wide use in previous literature. The results show that the presence of increasing...
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