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Zirconium Phosphate (ZrP) inside a composite membrane Nafion-ZrP was studied by combining wide angle X-ray diffraction (XRD) and high-resolution solid-state 31 P Nuclear Magnetic Resonance (NMR) under magic angle spinning conditions (MAS). We have, at first, investigated the physical features of ZrP powders that were prepared ex situ under different conditions leading to either amorphous or...
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