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Herein, we report a newly developed C60 fullerene‐bonded silica monolith in a capillary with unique retention behavior due to the structure of C60 fullerene. N‐Hydroxysuccinimide (NHS)‐conjugated C60 fullerene was successfully synthesized by a thermal coupling agent, perfluorophenyl azide (PFPA), and assigned by spectroscopic analyses. Then, NHS‐PFPA‐C60 fullerene was attached onto the surface of...
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